专利摘要:
The invention relates to the technology of producing fiberglass for optical fibers and improves the quality of compaction of powdered silica to a bulk density of 300 g / l without the use of a binder. According to this method of compaction of powdered silicon dioxide by pyrogenic means, it is first compacted in an open centrifuge, and then further compacted by a free-running piston in a centrifuge tank.
公开号:SU1667634A3
申请号:SU853947155
申请日:1985-08-06
公开日:1991-07-30
发明作者:Гинтер Херберт;Клингель Райнхард;Маннер Райнхард
申请人:Дегусса Аг (Фирма);
IPC主号:
专利说明:

This invention relates to a technology for producing glass fibers for optical fibers, which are obtained from extruded articles from pyrogenically produced silica powder.
The purpose of the invention is to improve the quality of compaction of powdered silica to a bulk density of 300 g / l without the use of a binder.
Example. Pyrogenically produced silica with a specific surface area of 50 g / m (trade name Aerosil OX 50 Degussa) was filled with centrifuge glasses with glass liners. The dimensions of the centrifuge glass cups are about 38 mm in internal diameter and about 100 mm in length with a volume of 100 cm. The centrifugal maximum centrifugal number achieved is 4000.
The initial density of the silicon dioxide is 20 g / l. This silicon dioxide is compacted by centrifugal force. With this product at
The average centrifugation rate of about 3200 is compacted to an average density of about 200 g / l. The acceleration time is 60 seconds.
This product, thus sealed, is immediately subsequently sealed with the help of a freely flying (moving) piston made of steel (P 7.86 kg / dm3). The piston diameter is 37 mm and its height is 20 mm.
The pistons are slid into glass cups until the pistons touch the pre-compacted product. Then the centrifuge is set in motion again, the pistons go outside and the pyrogenically produced silicon dioxide is further compacted.
The centrifugation time is about 5 minutes to obtain a homogeneous molded product.
After the piston is removed, it does not burst, but remains a homogeneous molded product.
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with
oh
xj o
SA
 WITH
3 16676344
The formula of the invention for a mass of 300 g / l without the use of a binder,
The method of compaction of the powder is last compacted first in the open
silicon dioxide, obtained by pyrogenic centrifuge, and then close the container
a path, characterized in that, in order to centrifuge freely moving in
enhancing the quality of compaction with a piston-5 with a piston and producing additional silicon dioxide by it to a bulk compaction.
权利要求:
Claims (1)
[1]
Claim
The method of compaction of powdered silicon dioxide obtained by pyrogenic method, characterized in that, in order to improve the quality of compaction of powdered * silica to a bulk density of 300 g / l without the use of a binder, the latter is first compacted in an open centrifuge, and then the centrifuge's container is closed with a freely moving in 5 with a piston and produce an additional seal.
类似技术:
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同族专利:
公开号 | 公开日
US4680043A|1987-07-14|
EP0172386A3|1988-02-17|
DE3581016D1|1991-02-07|
DE3429051C1|1986-02-13|
AT59626T|1991-01-15|
EP0172386A2|1986-02-26|
JPS6148423A|1986-03-10|
EP0172386B1|1991-01-02|
JPH0137328B2|1989-08-07|
引用文献:
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DE570813C|1930-12-07|1933-06-03|Wilhelm Mueller Dr|Process for compacting heated sinter masses|
US2304723A|1940-01-18|1942-12-08|Hammarbylampan Ab|Process for the manufacture of articles of sintered metallic constituents|
CH221356A|1940-01-18|1942-05-31|Hammarbylampan Ab|Process for the manufacture of articles from sintered metal or sintered hard alloy.|
US2960723A|1953-07-15|1960-11-22|Stark Howard John|Glass fiber forming machine|
US3888662A|1973-02-09|1975-06-10|Kennametal Inc|Method of centrifugally compacting granular material using a destructible mold|
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DE3217965A1|1982-05-13|1983-11-17|Standard Elektrik Lorenz Ag, 7000 Stuttgart|METHOD FOR PRODUCING FIBERGLASS FOCUS|
DE3240355C1|1982-11-02|1983-11-17|Heraeus Quarzschmelze Gmbh, 6450 Hanau|Process for the production of an elongated glass body with an inhomogeneous refractive index distribution|DE4142898A1|1991-12-23|1993-06-24|Sued Chemie Ag|Pyrogenic silica moulding used as catalyst support or catalyst - prepd. from paste in aq. alcoholic ammonia by moulding, drying and calcining|
DE4142902A1|1991-12-23|1993-06-24|Sued Chemie Ag|Producing mouldings for catalytic use from pyrogenic silicic acid - by hydrothermally treating initially moulded body with ammonia contg. solution|
US6156285A|1998-11-12|2000-12-05|Dow Corning Corporation|Method for densifying particulate silica|
DE19936478A1|1999-08-03|2001-02-15|Degussa|Sintered materials|
DE102006058813A1|2006-12-13|2008-06-19|Wacker Chemie Ag|Process for the preparation of stable, highly pure moldings from fumed metal oxides without the addition of binders|
DE102006058800A1|2006-12-13|2008-06-19|Wacker Chemie Ag|Process for the preparation of catalysts and their use for the gas-phase oxidation of olefins|
DE102006058799A1|2006-12-13|2008-06-19|Wacker Chemie Ag|Process for the preparation of stable binder-free high purity moldings from metal oxides and their application|
US10139296B1|2017-05-05|2018-11-27|Richard AGOSTINELLI|Centrifuge calibration apparatus|
法律状态:
优先权:
申请号 | 申请日 | 专利标题
DE3429051A|DE3429051C1|1984-08-07|1984-08-07|Process for the production of powders from powdery, pyrogenic silicon dioxide|
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